About the Instrument:
The JNM-ECZ600R/M3 is a 600 MHz NMR spectrometer from JEOL, a high-resolution instrument designed for advanced analytical applications, particularly in solid-state and liquid-state NMR. It uses a superconducting magnet, providing high sensitivity and resolution for detailed structural analysis of molecules.
Key Features and Capabilities:
High Field Strength: The instrument utilizes a 14.09 Tesla magnet, corresponding to a 600 MHz frequency for 1H.
Solid-State and Liquid-State NMR: It's capable of performing both solid-state and liquid-state NMR experiments.
Multiple Probes: The JNM-ECZ600R/M3 is equipped with a variety of probes, including:
Solid-state probes: 3.2 mm and 1 mm HX MAS probes for solid-state analysis, with variable temperature capabilities and fast rotation speeds.
Liquid-state probes: 5 mm FG/RO probe for liquid phase measurements, with automatic frequency tuning
.
Broadband probes: TH5 probe for 1H, 19F, 15N, and 31P nuclei, and Royal Probe for 15N to 31P.
Smart Transceiver System (STS): The instrument utilizes JEOL's STS technology for high-precision and stable RF control
.
Multi-sequencer: The multi-sequencer allows for complex and multi-dimensional NMR experiments with precise control of multiple RF sources
.
Temperature Control: Variable temperature control, allowing experiments from -100 to +150°C.
Automatic Sample Changer: An automatic sample changer for efficient sample analysis.
Software: The instrument comes with NMR software for data processing and analysis.
Usage:
Structural Analysis: Determining the structure of small molecules and proteins in solution.
Solid-State NMR: Studying the structure and dynamics of materials in the solid state.
Variable Temperature Studies: Performing NMR experiments at different temperatures for studying dynamic processes.
Reaction Monitoring: Tracking the progress of chemical reactions in real-time.
Material Science: Characterizing the chemical and physical properties of materials.